Original Research
Growth and characterization of DL-Norleucine maleate crystals
A. Z. Bazeera
a
D. Muthuraj
b
A. S. Mohamed
c
S. C. V. Durai
d
M. A. Nashrine

aDepartment of Physics, Sadakathullah Appa College, Tirunelveli, Tamilnadu,

India

bDepartment of Physics, M.D.T.Hindu College, Tirunelveli, Tamilnadu, India

cDepartment of Chemistry, Sadakathullah Appa College, Tirunelveli, Tamilnadu, India

dDepartment of Physics, JP College of Arts & Science, Tenkasi, Tamilnadu, India eDepartment of Physics, Sadakathullah Appa College, Tirunelveli, Tamilnadu,

India, Affiliated to Manonmaniam Sundaranar University, Abishekapatti,

Tirunelveli, Tamilnadu, India


Journal of Ovonic Research 2022, 18(2),195-204; https://doi.org/10.15251/JOR.2022.182.195
Submitted:Nov 29, 2021
Accepted:Mar 28, 2022
Published:Apr 12, 2022
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Cite This Article
A. Z. Bazeera ,D. Muthuraj ,A. S. Mohamed ,S. C. V. Durai ,M. A. Nashrine . (2022). Journal of Ovonic Research. Growth and characterization of DL-Norleucine maleate crystals, 18(2), ,195-204. https://doi.org/10.15251/JOR.2022.182.195
Abstract

To obtain the single crystals of DL-Norleucine Maleate (DLNM), slow evaporation solution growth technique was used. The good crystalline quality of the crystal was validated by the diffraction peaks of the Powder X-Ray diffraction techniques. The functional groups which are present in the crystal were validated by FTIR and FT Raman method. Density functional theory (DFT) computation gives optimized structure parameters of DLNM molecule. The compound is changeless thermally up to 160°C and it is illustrated by TG-DTA thermal studies. The composition of the DLNM crystal was studied by EDAX spectroscopy. NMR spectral and chemical shifts ofthe grown crystal of DLNM were analyzed. The study of Vickers micro hardness study leads to the hardness number (HV) evaluation and work hardening coefficient. Various dielectric parameters like AC conductivity, dielectric constant and loss energy of the sample were determined from the dielectric studies.

©2026 by the authors. Submitted for possible open access publication under the terms and conditions of the Creative Commons Attribution (CC BY) license (http://creativecommons.org/licenses/by/4.0/).
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