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Northeast Petroleum University, Department of petroleum and chemical
engineering, Qinhuangdao 066004, Hebei Province, China
Journal of Ovonic Research 2024, 20(3),357-364; https://doi.org/10.15251/JOR.2024.203.357
Rice grain-shaped high Mn-doped anatase TiO2(TMO) nanocrystals have been fabricated through redox method at room temperature using several simple chemical reagents. The samples were characterized by X-ray diffraction (XRD), X-ray photoelectron spectroscopy(XPS), scanning electron microscopy(SEM), transmission electron microscopy and High-resolution transmission electron microscopy (TEM & HRTEM). It indicates that the manganese element was successfully incorporated into the anatase TiO2 nanostructure, and the atomic Mn-to-Ti could reach up to 18.2%. We also analyzed the merits and weaknesses of the nanostructured TMO in electrochemistry by dint of some relevant measures. And the cause of influence on the TMO electrochemical properties was briefly discussed.
